Please use this identifier to cite or link to this item: http://earsiv.odu.edu.tr:8080/xmlui/handle/11489/3202
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dc.contributor.authorBagdatli, Emine-
dc.contributor.authorGunkara, Omer T.-
dc.contributor.authorOcal, Nuket-
dc.date.accessioned2022-09-07T06:51:58Z-
dc.date.available2022-09-07T06:51:58Z-
dc.date.issued2013-
dc.identifier.urihttp://doi.org/10.1016/j.jorganchem.2013.04.055-
dc.identifier.urihttp://earsiv.odu.edu.tr:8080/xmlui/handle/11489/3202-
dc.description.abstractNew copper(II) and palladium(II) complexes were synthesized by the interaction of metal acetates and azo-, bisazo-5-pyrazolones in a methanolic medium. The mononuclear copper(II) and palladium(II) complexes were obtained from the ligands, HAP/HL1a-b and HAP/HL2 (Azo-5-Pyrazolone Ligand), and the binuclear copper(II) complexes were obtained from the ligands, HBAP/HL2a and HBAP/HL1c (BisAzo-5-Pyrazolone Ligand). The resulting complexes were characterized on the basis of spectroscopic techniques such as infrared, mass spectra, nuclear magnetic resonance and UV-visible absorption spectra as well as thermal analyses. The spectral data show that the ligands coordinated via the carbonyl oxygen of 5-pyrazolone and via the azo group of the nitrogen atoms of the azo-, bisazo-5-pyrazolones, except for the complex [Pd(HL1a)(2)] which coordinated from the carbonyl oxygen of 5-pyrazolone and the hydroxyl oxygen of the azo-substituted aromatic ring. (C) 2013 Elsevier B. V. All rights reserved.en_US
dc.language.isoengen_US
dc.publisherELSEVIER SCIENCE SAPO BOX 564, 1001 LAUSANNE, SWITZERLANDen_US
dc.relation.isversionof10.1016/j.jorganchem.2013.04.055en_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectCopper complex Palladium complex Azo-, bisazo-5-pyrazolone bisazo-5-pyrazolone liganden_US
dc.titleSynthesis and characterization of new copper(II) and palladium(II) complexes with azo-, bisazo-5-pyrazolonesen_US
dc.typearticleen_US
dc.relation.journalJOURNAL OF ORGANOMETALLIC CHEMISTRYen_US
dc.contributor.departmentOrdu Üniversitesien_US
dc.contributor.authorID0000-0003-3528-5045en_US
dc.identifier.volume740en_US
dc.identifier.startpage33en_US
dc.identifier.endpage40en_US
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