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http://earsiv.odu.edu.tr:8080/xmlui/handle/11489/2498| Title: | MICROWAVE-ASSISTED SYNTHESIS |
| Authors: | Bekdemir, Yunus Gediz Erturk, Aliye Ordu Üniversitesi 0000-0003-0831-7056 |
| Keywords: | SULFAMIDE1,1-DIOXIDESTHERMOLYSISCHEMISTRYACID Sulfamidesamine-exchange reactionsmicrowave irradiation |
| Issue Date: | 2014 |
| Publisher: | TAYLOR & FRANCIS LTD2-4 PARK SQUARE, MILTON PARK, ABINGDON OR14 4RN, OXON, ENGLAND |
| Abstract: | Microwave-assisted synthesis of some substituted open-chain and cyclic sulfamides, by amine-exchange reaction, was studied in a modified domestic microwave oven. Reaction times and yields under microwave radiation were compared with classical heating. Synthesis of the sulfamides under microwave irradiation gave better yields with the desired compounds, and in considerably reduced reaction times, than those obtained by classical heating. [Supplementary materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfer, and Silicon and the Related Elements for the following free supplemental files: Additional figures.] |
| URI: | http://doi.org/10.1080/10426507.2013.819868 http://earsiv.odu.edu.tr:8080/xmlui/handle/11489/2498 |
| Appears in Collections: | Kimya |
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