Please use this identifier to cite or link to this item: http://earsiv.odu.edu.tr:8080/xmlui/handle/11489/4525
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dc.contributor.authorKelebekli, Latif-
dc.contributor.authorCelik, Murat-
dc.contributor.authorKara, Yunus-
dc.date.accessioned2024-03-15T11:23:59Z-
dc.date.available2024-03-15T11:23:59Z-
dc.date.issued2010-
dc.identifier.citationKelebekli, L., Celik, M., Kara, Y. (2010). A novel and stereospecific synthesis of aminocyclitol: N-tosyldihydroconduramine E2. J. Chem. Res, 1, 54-56. https://doi.org/10.3184/030823410X12628681698796en_US
dc.identifier.issn1747-5198-
dc.identifier.issn2047-6507-
dc.identifier.urihttp://dx.doi.org/10.3184/030823410X12628681698796-
dc.identifier.urihttps://www.webofscience.com/wos/woscc/full-record/WOS:000275412500016-
dc.identifier.urihttp://earsiv.odu.edu.tr:8080/xmlui/handle/11489/4525-
dc.descriptionWoS Categories: Chemistry, Multidisciplinaryen_US
dc.descriptionWeb of Science Index: Science Citation Index Expanded (SCI-EXPANDED); Index Chemicus (IC); Current Chemical Reactions (CCR-EXPANDED)en_US
dc.descriptionResearch Areas: Chemistryen_US
dc.description.abstractA stereospecific synthesis of N-tosyldihydroconduramine E2, a new aminocyclitol, has been synthesised starting from cyclohexa-1,3-diene. The photooxygenation of cyclohexa-1,3-diene afforded the bicyclic endoperoxide. Reduction of the endoperoxide with thiourea and then reaction of the bis-carbamate with p-TsNCO followed by a palladium-catalysed ionisation/cyclisation reaction, gave a vinyl oxazolidin-2-one. Oxidation of the double bond in the oxazolidin-2-one with KMnO4 followed by acetylation, gave the oxazolidinone-diacetates. Hydrolysis of the oxazolidinone ring and removal of the acetate groups gave the desired aminocyclitol, N-tosyldihydroconduramine E2.en_US
dc.description.sponsorshipTUBITAK (The Scientific and Technical Research Council of Turkey) [TBAG-105T162]en_US
dc.language.isoengen_US
dc.publisherSAGE PUBLICATIONS LTD-LONDONen_US
dc.relation.isversionof10.3184/030823410X12628681698796en_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectN-tosyldihydroconduramine E2, conduramine, aminocyclitol, endoperoxideen_US
dc.subjectAMINOCYCLOPENTITOL GLYCOSIDASE INHIBITORS, ASYMMETRIC INDUCTION, RADICAL CYCLIZATION, CYCLITOLS, PUREen_US
dc.titleA novel and stereospecific synthesis of aminocyclitol: N-tosyldihydroconduramine E2en_US
dc.typearticleen_US
dc.relation.journalJOURNAL OF CHEMICAL RESEARCHen_US
dc.contributor.departmentOrdu Üniversitesien_US
dc.identifier.issue1en_US
dc.identifier.startpage54en_US
dc.identifier.endpage56en_US
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